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. 2017 Jun 27;15(7):202. doi: 10.3390/md15070202

Table 2.

1H NMR spectroscopic data of compounds 13 (400 MHz, CDCl3) and 4 (400 MHz, DMSO-d6).

No. 1 2 3 4
2 - 4.87 d (11.2) - 5.53 d (10.4)
3 2.16 br s 5.26 dd (10.8, 0.8) 5.21 s 4.99 d (10.4)
5 3.04 q (10.8) 2.34 m 2.09 m 2.18 m
1.67 m - 1.78 m -
6 2.00 dd (9.6, 2.4) 1.92 m 1.54 m 1.97 m
1.54 m 1.63 m 1.51 m 1.42 m
7 3.80 dd (9.2, 5.6) 2.65 t (4.0) 3.52 dd (9.2, 3.2) 3.01 dd (10.0, 2.8)
9 1.50 m 2.13 m 1.64 m 1.73 m
1.25 m 0.93 m 1.47 m 1.49 m
10 2.05 m 2.27 m 2.17 m 1.62 m
1.90 m 1.87 m 1.86 m 1.34 m
11 5.15 t (7.6) 5.11 dd (9.6, 5.6) 4.99 t (6.8) 3.13 d (10.4)
13 2.28 br d (13.2) 2.22 m 2.28 m 1.70 m
1.84 m 1.95 m - 1.49 m
14 2.61 td (13.2, 2.1) 1.69 m 2.56 m 2.45 m
2.12 m - - 1.91 m
16 4.90 br s 3.89 d (10.4) - -
- 3.75 d (10.4) - -
17 2.08 s 1.43 s 1.94 s 1.73 s
18 1.35 s 1.84 s 1.40 s 1.77 s
19 1.03 s 1.27 s 1.61 s 0.98 s
20 1.69 s 1.57 s 1.67 s 0.98 s