Table 2.
Comparison of the MSPE + UV method with other analytical techniques for extraction and determination of PQ.
| Sample | Extraction and detection technique | Extract method and extractant | Linear range (μg/L) | Limits of detection (μg/L) | Ref. |
|---|---|---|---|---|---|
| Urine | UV-Vis | — | 1000–1500 | — | [8] |
| Human blood | UV-Vis | LLE dichloromethane | 84.1–841 | 89.1 | [24] |
| Human blood and urine | GC | — | 1 × 103–7 × 104 | — | [9] |
| Plasma and urine | GC-MS | SPE C18 cartridge |
100–50000 | 50 | [10] |
| Urine | GC-MS | HS-SPME fiber |
10–1000 | 0.1 | [11] |
| Plasma | HPLC-UV | — | 2 × 105–5 × 108 | — | [12] |
| Whole blood | HPLC-UV | — | 300–30000 | 26 | [25] |
| Human plasma | HPLC- UV | SPE Xtimate C18 column |
20–1 × 104 | 10 | [26] |
| Urine | HPLC-MS | DSPE Carbon nanotube |
3.75–375.0 | 0.94 | [14] |
| Plasma and urine | UV-Vis | SPE SiO2@Fe3O4 |
15–400 | 4.7 | This work |
HS-SPME: headspace solid phase microextraction; DSPE: dispersive solid phase extraction.