Skip to main content
. Author manuscript; available in PMC: 2017 Nov 9.
Published in final edited form as: J Am Chem Soc. 2016 Nov 1;138(44):14554–14557. doi: 10.1021/jacs.6b09653

Table 1.

Development of the Transient Directing Groupa, b

graphic file with name nihms877177f2.jpg
a

Conditions: 1a (0.2 mmol), 4-CO2MePhI (0.4 mmol), Pd(OAc)2 (10 mol%), TDG (20 mol%), AgTFA (0.4 mmol), HFIP/HOAc = 19/1 (1.0 mL), H2O (2.0 mmol), 120 °C, 12 h.

b

Yields were determined by 1H NMR analysis of the crude reaction mixture using CH2Br2 as the internal standard.