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. 2017 Jul 31;7:6909. doi: 10.1038/s41598-017-06947-w

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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(a) Possible equilibria and routes for generating cis-3 in solution. (b) Kinetics of aqueous dissolution of UV-irradiated crystals of 3, measured in the dark. Crystals of 3 were irradiated with 365 nm LED light (344 mW/cm²) at 37 °C for 3 h. The UV-irradiated crystals and unirradiated crystals were each shaken with phosphate buffer in the dark at 37 °C for 1 h. Data are the mean ± SD of three individual experiments. The asterisk indicates a significant difference (*p < 0.05) from the unirradiated crystals according to the unpaired, two-sided Student’s t-test.