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. 2017 Aug 2;5:58. doi: 10.3389/fchem.2017.00058

Table 1.

Phytochemical analysis and Identification of major compounds in various fractions of Polygonum hydropiper.

RT Height Height % Area Area % Area sum % Base peak m/z Width Compound name
(A)
10.341 818,728 33.34 3E + 06 31.32 7.89 120 0.198 2,3-dihydro benzofuran
18.807 582,512 23.72 1E + 06 14.06 3.54 43.1 0.09 Humulene oxide
19.222 570,159 23.22 1E + 06 14.61 3.68 67.1 0.087 (−)Caryophyllene oxide
19.359 557,134 22.69 1E + 06 12.61 3.18 203.1 0.084 2H-Cyclopropa[g]benzofuran
24.024 2E + 06 100 9E + 06 100 25.2 68.1 0.161 Neophytadiene
24.835 637,992 25.98 2E + 06 25.56 6.44 81.1 0.157 3,7,11,15-Tetramethyl-2-hexadecen-1-ol
25.411 1E + 06 42.45 4E + 06 42.52 10.71 81.1 0.161 3,7,11,15-Tetramethyl-2-hexadecen-1
31.064 468,188 19.07 1E + 06 13.53 3.41 67.1 0.1 (E,E)-Methyl linolelaidate
31.215 637,675 25.97 2E + 06 23.16 5.84 79 0.147 11,14,17-Eicosatrienoic acid, methyl ester
31.506 858,095 34.94 3E + 06 32.32 8.14 71 0.167 Hexa-hydro-farnesol
(B)
6.591 131,777 4.41 392,385 2.78 0.95 44.1 0.09 Monomethyl malonate
9.35 609,951 20.43 1,481,562 10.5 3.57 95.1 0.107 endo-Borneol
9.966 501,142 16.79 2,336,018 16.55 5.64 110 0.248 Pyrocatechol
10.395 3E + 06 100 14,111,231 100 34.05 120 0.224 Coumaran
12.592 1E + 06 46.29 7,022,887 49.77 16.94 150 0.204 p-Vinylguaiacol
15.294 2E + 06 54.56 5,540,018 39.26 13.37 95.1 0.131 Alpha santolina alcohol
18.613 430,440 14.42 794,117 5.63 1.92 91 0.067 Humulen
19.373 2E + 06 73.74 5,020,261 35.58 12.11 203.1 0.084 Cyclopropa[g]benzofuran
39.64 2E + 06 56.68 4749427 33.66 11.46 149 0.107 1,2-Benzenedicarboxylic acid
(C)
15.702 5,894,271 48.37 13,241,763 37.21 5.13 93.1 0.094 Humulene
18.331 6,998,724 57.44 17,735,706 49.84 6.87 79.1 0.1 beta-Caryophyllene epoxide
18.857 12,184,878 100 35,584,370 100 13.79 67.1 0.131 Humulene oxide
19.269 5,604,173 45.99 19,882,595 55.87 7.7 67.1 0.131 Caryophyllene oxide
22.179 4,861,002 39.89 18,735,011 52.65 7.26 109.1 0.147 Drimenol
25.448 3,237,750 26.57 12697359 35.68 4.92 81.1 0.147 3,7,11,15-Tetramethyl-2-hexadecen-1-ol
26.778 5,389,458 44.23 19,824,080 55.71 7.68 74 0.144 Methyl palmitate
31.118 4,228,256 34.7 14,158,473 39.79 5.49 67.1 0.124 Methyl linoleate
31.276 6,219,883 51.05 22,845,516 64.2 8.85 79 0.214 9,12,15-Octadecatrienoic acid, methyl ester
(D)
6.553 475,471 6.94 1,106,068 5.59 2.31 99 0.141 M-Pyrol
18.328 405,020 5.91 800,942 4.05 1.67 79.1 0.07 beta-Caryophyllene epoxide
18.837 582,101 8.49 1,480,419 7.48 3.09 67.1 0.124 Humulene oxide
20.458 417,424 6.09 1,254,667 6.34 2.62 55.1 0.127 Globulol
25.438 640,981 9.35 2,449,409 12.38 5.12 81 0.164 3,7,11,15-Tetramethyl-2-hexadecen-1-ol
26.704 2E + 06 22.92 5,009,852 25.32 10.47 74 0.127 Methyl palmitate
30.639 1E + 06 18.56 3,462,672 17.5 7.23 67.1 0.107 9,12-Octadecadienoic acid, methyl ester
30.776 2E + 06 24.25 5,004,849 25.3 10.46 79 0.121 Methyl linolenate
31.034 571,769 8.34 1,820,926 9.2 3.8 71.1 0.144 Phytol
(E)
9.356 6E + 06 64.28 14,136,851 26.65 14.21 95.1 0.131 Borneol
10.408 9E + 06 100 53,040,523 100 53.32 120 0.352 Coumaran
12.601 5E + 06 53.22 17,351,644 32.71 17.44 150 0.238 p-Vinylguaiacol
14.296 337,994 3.85 770,318 1.45 0.77 111 0.077 Cyclohexanebutanal
15.287 1E + 06 15.93 4,429,002 8.35 4.45 95.1 0.124 alpha-santolina alcohol
15.786 1E + 06 14.16 2,865,277 5.4 2.88 91 0.124 1(7),5,8-o-Menthatriene
18.127 305,613 3.48 561,559 1.06 0.56 91 0.067 8-Isopropenyl-1,3,3,7-tetramethyl-
18.599 439,654 5.01 976,253 1.84 0.98 79.1 0.087 Bicyclo[3.3.0]octan-2-one, 7-ethylidene
19.235 689,601 7.86 1,354,090 2.55 1.36 67.1 0.077 Caryophyllene oxide
19.366 1E + 06 13.11 3,986,649 7.52 4.01 203.1 0.124 Aristolone

A) Crude methanolic extract (Ph.Cr), B) Ethyl acetate fraction (Ph.EtAc), C) n-Hexane fraction (Ph.Hex), D) Chloroform fraction (Ph.Chf), E) Butanol fraction (Ph.Bt).