Table 4. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source	23-ID-B, APS
Wavelength (Å)	1.033200
Temperature (K)	100
Detector	EIGER
Crystal-to-detector distance (mm)	200.0
Rotation range per image (°)	0.2
Total rotation range (°)	200
Exposure time per image (s)	0.2
Space group	C2
a, b, c (Å)	111.72, 114.74, 79.97
α, β, γ (°)	90.0, 109.8, 90.0
Resolution range (Å)	1.65 (1.75–1.65)
Total No. of reflections	431338 (70385)
No. of unique reflections	111796 (17858)
Completeness (%)	98.2 (97.2)
Multiplicity	3.86 (3.94)
〈I/σ(I)〉	22.08 (3.16)
R r.i.m. (%)	3.6 (59.1)