Table 1.
Crystallographic data collection and refinement statistics
Values in parentheses are for the highest resolution shell.
| Data statistics | |
|---|---|
| Data collection | |
| PDB entry | 5VPN |
| Beamline | APS 21-IDG |
| Wavelength | 0.97856 Å |
| Resolutiona | 4.25 Å |
| Space group | P212121 |
| Unit cell | a = 133.6 Å |
| b = 138.1 Å | |
| c = 220.1 Å | |
| Rsym | 0.166 (0.899)b |
| Rpim | 0.075 (0.448) |
| CC½ | 0.919 |
| I/σa | 10.6 (1.4) |
| Completeness | 96.8% (98.2%) |
| Redundancy | 5.5 (4.6) |
| Refinement | |
| Rcryst | 0.215 |
| Rfree | 0.270 |
| Root mean square deviation | |
| Bond lengths | 0.003 Å |
| Bond angles | 0.614° |
| Ramachandran | |
| Most favored | 93.6% |
| Allowed | 6.1% |
| Outliers | 0.3% |
a The data have an I/σ > 2 in the outer shell at 4.4-Å resolution.
b Values in parentheses are statistics for the highest resolution shell, 4.4–4.25-Å resolution.