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. 2017 Aug 9;7:7697. doi: 10.1038/s41598-017-08100-z

Table 3.

1H and 13C NMR data for muriceidone A (4) in CDCl3.

Position δ C a δ H b (J in Hz) Position δ C a δ H b (J in Hz)
1 167.3, C 1′ 76.7, C
2 132.1, CH 6.19 (s) 2′ 59.5, CH 3.03 (s)
3 206.4, C 3′ 202.3, C
4 133.4, C 4′ 140.0, C
5 124.3, CH 6.26 (d, 6.6) 5′ 134.4, C
6 126.3, CH 6.54 (d, 6.6) 6′ 194.6, CH 10.61 (s)
7 147.5, C 7′ 157.4, C
8 117.1, CH 6.44 (s) 8′ 118.7, CH 7.49 (s)
9 138.3, C 9′ 162.4, C
10 55.7, C 10′ 129.3, C
11 36.0, CH 2.69 (dq, 6.6, 7.2) 11′ 29.6, CH 3.59 (dq, 6.6, 6.6)
12 23.0, CH3 1.13 (d, 6.6) 12′ 23.9, CH3 1.27 (d, 6.6)
13 23.5, CH3 1.17 (d, 7.2) 13′ 24.0, CH3 1.30 (d, 6.6)
14 15.1, CH3 2.31 (s) 14′ 28.4, CH3 1.87 (s)
15 24.1, CH3 1.83 (s) 15′ 14.3, CH3 2.69 (s)
OH-3′ 2.17 (br s)

aRecorded at 150 MHz. bRecorded at 600 MHz.