Table 3.
Position | δ C a | δ H b (J in Hz) | Position | δ C a | δ H b (J in Hz) |
---|---|---|---|---|---|
1 | 167.3, C | 1′ | 76.7, C | ||
2 | 132.1, CH | 6.19 (s) | 2′ | 59.5, CH | 3.03 (s) |
3 | 206.4, C | 3′ | 202.3, C | ||
4 | 133.4, C | 4′ | 140.0, C | ||
5 | 124.3, CH | 6.26 (d, 6.6) | 5′ | 134.4, C | |
6 | 126.3, CH | 6.54 (d, 6.6) | 6′ | 194.6, CH | 10.61 (s) |
7 | 147.5, C | 7′ | 157.4, C | ||
8 | 117.1, CH | 6.44 (s) | 8′ | 118.7, CH | 7.49 (s) |
9 | 138.3, C | 9′ | 162.4, C | ||
10 | 55.7, C | 10′ | 129.3, C | ||
11 | 36.0, CH | 2.69 (dq, 6.6, 7.2) | 11′ | 29.6, CH | 3.59 (dq, 6.6, 6.6) |
12 | 23.0, CH3 | 1.13 (d, 6.6) | 12′ | 23.9, CH3 | 1.27 (d, 6.6) |
13 | 23.5, CH3 | 1.17 (d, 7.2) | 13′ | 24.0, CH3 | 1.30 (d, 6.6) |
14 | 15.1, CH3 | 2.31 (s) | 14′ | 28.4, CH3 | 1.87 (s) |
15 | 24.1, CH3 | 1.83 (s) | 15′ | 14.3, CH3 | 2.69 (s) |
OH-3′ | 2.17 (br s) |
aRecorded at 150 MHz. bRecorded at 600 MHz.