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. Author manuscript; available in PMC: 2018 Apr 28.
Published in final edited form as: J Nat Prod. 2017 Mar 30;80(4):1141–1149. doi: 10.1021/acs.jnatprod.7b00108

Table 1.

13C NMR (100/125 MHz) Data for Compounds 1–4 and 8–12

no. 1a 2c 3a 4a 8c 9a 10a 11a 12b
1 173.1, C 174.9, C 173.2, C 171.5, C 173.4, C 168.9, C 169.5, C 169.2, C 176.8, C
2 99.0, C 98.8, C 98.8, C 106.4, C 98.4, C 100.2, C 99.0, C 96.6, C 96.9, C
3 179.5, C 180.7, C 178.9, C 186.5, C 180.9, C 199.0, C 199.7, C 180.7, C 201.2, C
4 40.3, CH 40.4, CH 39.9, CH 40.0, CH 40.7, CH 40.5, CH 42.2, CH 30.0, CH 38.1, CH
5 33.7, CH2 34.2, CH2 33.1, CH2 38.3, CH2 32.8, CH2 40.3, CH2 38.4, CH2 46.1, CH2 47.5, CH2
6 48.1, CH 48.1, CH 47.7, CH 77.8, C 48.5, CH 79.7, C 45.9, CH 78.0, C 210.9, C
7 210.7, C 210.2, C 210.5, C 209.1, C 209.5, C 207.2, C 211.6, C 215.3, C 170.2, C
8 58.5, CH 59.7, CH 58.5, CH 66.1, CH 53.2, CH 48.3, CH 34.4, CH2 43.9, CH2 122.6, CH
9 27.2, CH2 27.6, CH2 26.8, CH2 77.1, CH 36.2, CH2 55.9, CH 19.4, CH2 27.2, CH 149.8, CH
10 50.3, CH 49.7, CH 48.8, CH 50.6, CH 60.5, C 45.9, CH 44.6, CH 45.3, CH 47.8, CH
11 81.3, CH 80.9, CH 78.9, CH 72.2, CH 64.8, CH 67.0, CH 74.8, CH 71.7, CH 120.8, CH
12 76.0, C 78.5, C 77.6, C 76.8, C 75.4, C 88.6, C 88.5, C 84.9, C 141.0, C
13 73.7, C 27.7, CH 35.2, CH 26.7, CH 86.5, C 27.6, C 35.0, C 28.0, CH 32.5, CH
14 44.2, CH2 33.8, CH2 29.4, CH2 33.6, CH2 38.7, CH2 34.7, CH2 33.4, CH2 40.6, CH2 36.2, CH2
15 86.9, C 87.4, C 87.2, C 80.7, C 95.2, C 78.0, C 77.8, C 76.7, C 86.0, C
16 84.4, C 85.7, C 84.8, C 87.0, C 90.0, C 179.4, C 184.6, C 171.5, C 199.4, C
17 19.6, CH3 19.9, CH3 19.4, CH3 18.8, CH3 21.0, CH3 17.3, CH3 16.5, CH3 17.2, CH3 18.0, CH3
18 19.3, CH3 19.8, CH3 19.0, CH3 28.1, CH3 20.0, CH3 25.7, CH3 19.3, CH3 28.0, CH3 30.1, CH3
19 17.6, CH3 20.9, CH3 20.8, CH3 20.6, CH3 15.5, CH3 18.6, CH3 19.1, CH3 19.0, CH3 21.3, CH3
20 26.0, CH3 16.1, CH3 61.5, CH2 15.9, CH3 20.5, CH3 16.0, CH3 60.2, CH2 16.0, CH3 19.5, CH3
9-OCH3 56.9, CH3
a

Measured in DMSO-d6.

b

Measured in CD3OD.

c

Measured in CDCl3.