Table 2.
no. | 5a | 5Ba | 5Cb,d | 6c | 6Bc | 6Cb | 7a | 7Ba | 7Cb |
---|---|---|---|---|---|---|---|---|---|
1 | 172.7, C | 171.7, C | NDe | 177.3, C | 175.6, C | 164.3, C | 172.2, C | 171.3, C | 164.5, C |
2 | 98.1, C | 54.3, CH | 114.2, C | 99.7, C | 55.9, CH | 113.9, C | 97.9, C | 54.4 CH | 110.2,qC |
3 | 179.9, C | 106.4, C | 166.7, C | 182.7, C | 108.3, C | 167.7, C | 180.1, C | 106.4, C | 167.8, C |
4 | 35.8, CH | 42.3, CH | 36.5, CH | 37.5, CH | 43.7, CH | 36.5, CH | 35.9, CH | 42.4, CH | 36.6, CH |
5 | 37.9, CH2 | 36.3, CH2 | 39.2, CH2 | 39.6, CH2 | 38.3, CH2 | 38.9, CH2 | 38.1, CH2 | 36.3, CH2 | 39.2, CH2 |
6 | 77.6, C | 80.2, C | 78.2, C | 79.6, C | 82.6, C | 78.1, C | 77.7, C | 80.2, C | 78.3, C |
7 | 208.8, C | 200.3, C | 206.4, C | 210.1, C | 201.9, C | 206.6, C | 208.7, C | 200.1, C | 206.9, C |
8 | 66.9, CH | 68.3, CH | 63.0, CH | 68.7, CH | 70.1, CH | 63.5, CH | 66.4, CH | 67.7, CH | 64.0, CH |
9 | 66.9, CH | 67.6, CH | 70.2, CH | 68.9, CH | 70.1, CH | 73.8, CH | 67.0, CH | 67.7, CH | 70.3, CH |
10 | 53.5, CH | 52.8, CH | 49.6, CH | 55.4, CH | 54.4, CH | 49.2, CH | 54.4, CH | 53.5, CH | 50.8, CH |
11 | 71.9, CH | 71.7, CH | 73.8, CH | 74.7, CH | 74.5, CH | 70.0, CH | 74.8, CH | 74.4, CH | 75.9, CH |
12 | 78.0, C | 77.6, C | 77.3, C | 79.3, C | 78.8, C | 81.2, C | 75.2, C | 75.1, C | 73.1, C |
13 | 26.8, CH | 27.0, CH | 28.9, CH | 36.6, CH | 36.8, CH | 33.7, CH | 73.1, C | 73.1, C | 76.7, C |
14 | 33.7, CH2 | 31.7, CH2 | 34.2, CH2 | 30.6, CH2 | 28.7, CH2 | 29.6, CH2 | 44.0, CH2 | 42.4, CH2 | 45.1, CH2 |
15 | 84.5, C | 83.1, C | 81.6, C | 86.5, C | 84.6, C | 76.0, C | 84.0, C | 82.7, C | 81.7, C |
16 | 84.5, C | 83.7, C | 84.1, C | 86.8, C | 85.8, C | 84.3, C | 83.7, C | 83.2, C | 83.6, C |
17 | 19.0, CH3 | 11.2, CH3 | 17.5, CH3 | 19.9, CH3 | 12.2, CH3 | 17.9, CH3 | 18.9, CH3 | 11.3, CH3 | 17.5, CH3 |
18 | 27.2, CH3 | 22.6, CH3 | 27.7, CH3 | 28.0, CH3 | 22.9, CH3 | 27.4, CH3 | 27.1, CH3 | 22.6, CH3 | 27.7, CH3 |
19 | 20.4, CH3 | 20.6, CH3 | 20.8, CH3 | 21.6, CH3 | 21.2, CH3 | 20.8, CH3 | 17.3, CH3 | 17.4, CH3 | 17.3, CH3 |
20 | 15.8, CH3 | 15.9, CH3 | 16.0, CH3 | 63.8, CH2 | 63.3, CH2 | 64.2, CH2 | 25.6, CH3 | 25.6, CH3 | 25.7, CH3 |
Measured in DMSO-d6.
Measured in CDCl3.
Measured in CD3OD.
Obtained from HSQC and HMBC.
ND: not detected.