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. Author manuscript; available in PMC: 2018 Apr 28.
Published in final edited form as: J Nat Prod. 2017 Mar 30;80(4):1141–1149. doi: 10.1021/acs.jnatprod.7b00108

Table 2.

13C NMR (100/125 MHz) Data for Compounds 5, 5B, 5C, 6, 6B, 6C, 7, 7B, and 7C

no. 5a 5Ba 5Cb,d 6c 6Bc 6Cb 7a 7Ba 7Cb
1 172.7, C 171.7, C NDe 177.3, C 175.6, C 164.3, C 172.2, C 171.3, C 164.5, C
2 98.1, C 54.3, CH 114.2, C 99.7, C 55.9, CH 113.9, C 97.9, C 54.4 CH 110.2,qC
3 179.9, C 106.4, C 166.7, C 182.7, C 108.3, C 167.7, C 180.1, C 106.4, C 167.8, C
4 35.8, CH 42.3, CH 36.5, CH 37.5, CH 43.7, CH 36.5, CH 35.9, CH 42.4, CH 36.6, CH
5 37.9, CH2 36.3, CH2 39.2, CH2 39.6, CH2 38.3, CH2 38.9, CH2 38.1, CH2 36.3, CH2 39.2, CH2
6 77.6, C 80.2, C 78.2, C 79.6, C 82.6, C 78.1, C 77.7, C 80.2, C 78.3, C
7 208.8, C 200.3, C 206.4, C 210.1, C 201.9, C 206.6, C 208.7, C 200.1, C 206.9, C
8 66.9, CH 68.3, CH 63.0, CH 68.7, CH 70.1, CH 63.5, CH 66.4, CH 67.7, CH 64.0, CH
9 66.9, CH 67.6, CH 70.2, CH 68.9, CH 70.1, CH 73.8, CH 67.0, CH 67.7, CH 70.3, CH
10 53.5, CH 52.8, CH 49.6, CH 55.4, CH 54.4, CH 49.2, CH 54.4, CH 53.5, CH 50.8, CH
11 71.9, CH 71.7, CH 73.8, CH 74.7, CH 74.5, CH 70.0, CH 74.8, CH 74.4, CH 75.9, CH
12 78.0, C 77.6, C 77.3, C 79.3, C 78.8, C 81.2, C 75.2, C 75.1, C 73.1, C
13 26.8, CH 27.0, CH 28.9, CH 36.6, CH 36.8, CH 33.7, CH 73.1, C 73.1, C 76.7, C
14 33.7, CH2 31.7, CH2 34.2, CH2 30.6, CH2 28.7, CH2 29.6, CH2 44.0, CH2 42.4, CH2 45.1, CH2
15 84.5, C 83.1, C 81.6, C 86.5, C 84.6, C 76.0, C 84.0, C 82.7, C 81.7, C
16 84.5, C 83.7, C 84.1, C 86.8, C 85.8, C 84.3, C 83.7, C 83.2, C 83.6, C
17 19.0, CH3 11.2, CH3 17.5, CH3 19.9, CH3 12.2, CH3 17.9, CH3 18.9, CH3 11.3, CH3 17.5, CH3
18 27.2, CH3 22.6, CH3 27.7, CH3 28.0, CH3 22.9, CH3 27.4, CH3 27.1, CH3 22.6, CH3 27.7, CH3
19 20.4, CH3 20.6, CH3 20.8, CH3 21.6, CH3 21.2, CH3 20.8, CH3 17.3, CH3 17.4, CH3 17.3, CH3
20 15.8, CH3 15.9, CH3 16.0, CH3 63.8, CH2 63.3, CH2 64.2, CH2 25.6, CH3 25.6, CH3 25.7, CH3
a

Measured in DMSO-d6.

b

Measured in CDCl3.

c

Measured in CD3OD.

d

Obtained from HSQC and HMBC.

e

ND: not detected.