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. 2017 Aug 17;8:297. doi: 10.1038/s41467-017-00099-1

Fig. 6.

Fig. 6

Synthesis of ±-5-methylhentriacontane. a LiAlH4, Et2O (95%); b Tf2O, pyridine, CH2Cl2 (quantitative); c tert-Butyldimethyl(tridec-12-ynyloxy)silane, n-BuLi, THF (74%); d AcCl, dry MeOH (96%); e Tf2O, pyridine, CH2Cl2 (quantitative); f hexadecynyllithium, THF (49%); g 10% Pd/C, H2, hexane (~quantitative)