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LC-MS/MS conditions for the detection of NIV, D3G, and DON.
| Analyte | Precursor Ion | Product Ion | Retention Time (min) |
|---|---|---|---|
| NIV (C15H20O7) |
371.1 [C15H20O7+CH3COO]− |
280.8 | 1.74–1.81 |
| 310.7 | 1.71–1.87 | ||
| 59.0 | 1.74–1.87 | ||
| D3G (C21H30O11) |
517.1 [C21H30O11+CH3COO]− |
456.9 | 2.28–2.48 |
| 426.9 | 2.29–2.49 | ||
| 58.9 | 2.28–2.48 | ||
| DON (C15H20O6) |
355.1 [C15H20O6+CH3COO]− |
294.8 | 2.86–3.00 |
| 264.8 | 2.86–3.00 | ||
| 58.9 | 2.86–3.00 |
