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. 2017 Aug 10;15(8):249. doi: 10.3390/md15080249

Table 1.

13C and 1H-NMR data of compounds 1 and 2 in CDCl3.

No. 1 2
13C 1H (J in Hz) 13C 1H (J in Hz)
1 167.0 s - - 166.5 s - -
2 119.0 s - - 128.2 s - -
3 106.0 d - 6.38 brs 140.0 d - 6.63 brd (6.7)
4 156.4 s - - 23.8 t a 2.34 m
- - - - - - - b 2.21 ddd (3.1, 6.7, 17.7)
5 38.1 t - 3.28 s (2H) 81.9 d - 4.30 dd (3.1, 12.9)
6 130.9 s - - 38.9 s - -
7 127.2 d - 5.24 m 31.8 t α 1.56 m
- - - - - - - β 1.30 m
8 26.3 t - 2.16 m (2H) 17.4 t - 1.51 m (2H)
9 39.2 t - 2.06 m (2H) 37.8 t α 0.97 dt (3.1, 12.6)
- - - - - - - β 1.67 m
10 139.7 s - - 38.9 s - -
11 124.9 d - 5.24 m 46.6 d - 1.73 dd (2.6, 11.3)
12 75.9 d - 4.56 dt (8.4, 5.9) 17.5 t α 1.55 m
- - - - - - - β 1.47 m
13 39.4 t a 2.58 dd (5.9, 15.0) 41.6 t α 1.65 m
- - - b 2.23 m - - β 1.70 m
14 139.8 s - - 73.0 s - -
15 119.2 d - 5.33 m 58.8 d - 1.05 brs
16 29.9 t - 2.16 m (2H) 26.0 t a 1.68 m
- - - - - - - b 1.54 m
17 24.6 t - 2.48 t (7.5) (2H) 28.4 t a 2.44 m
- - - - - - - b 2.39 m
18 124.5 s - - 125.4 s - -
19 110.9 d - 6.26 brs 110.9 d - 6.29 brs
20 142.7 d - 7.34 brs 142.6 d - 7.35 brt (1.5)
21 138.9 d - 7.21 brs 138.6 d - 7.25 brs
22 68.3 t a 4.39 d (13.0) 30.5 q - 1.18 s
- - - b 4.20 d (13.0) - - - -
23 16.7 q - 1.70 brs 15.9 q - 1.03 s
24 15.9 q - 1.60 brs 17.4 q - 0.87 s
25 147.7 d - 7.96 brs 16.9 q - 1.92 s