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Assay validation parameters of MDA quantification in human plasma
| Sample Preparation | Concentration (μM) | Precision | Accuracy (%) | Recovery (%) | Matrix Effects (%) | Process Efficiency (%) | |
| RSD1 (%) | RSD2 (%) | ||||||
| Free MDA | 0.24 | 12.8 | 24.9 | 101 | 67 | 104 | 69 |
| Total MDA | 12.8 | 2.9 | 3.0 | 107 | 70 | 91 | 64 |
RSD1, intra-day precision (n = 5); RSD2, inter-day precision over three consecutive days (n = 15).
