| Crystal data |
| Chemical formula |
C15H18N2O2S |
|
M
r
|
290.37 |
| Crystal system, space group |
Orthorhombic, P212121
|
| Temperature (K) |
173 |
|
a, b, c (Å) |
5.5322 (2), 7.8707 (3), 32.9092 (14) |
|
V (Å3) |
1432.94 (10) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.23 |
| Crystal size (mm) |
0.28 × 0.10 × 0.09 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2014 ▸) |
|
T
min, T
max
|
0.690, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
11035, 2536, 2302 |
|
R
int
|
0.046 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.034, 0.072, 1.04 |
| No. of reflections |
2536 |
| No. of parameters |
181 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.20, −0.19 |
| Absolute structure |
Flack x determined using 839 quotients [(I
+) − (I
−)]/[(I
+) + (I
−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.05 (5) |
