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. Author manuscript; available in PMC: 2017 Sep 7.
Published in final edited form as: Synthesis (Stuttg). 2016 Apr 20;48(15):2376–2384. doi: 10.1055/s-0035-1561433

Scheme 2.

Scheme 2

Synthesis of 1-aryl 2-chloro-2,4,4,4-tetrafluorobutane-1,3-diones 3-6 by stepwise chlorination/fluorination of trifluoromethylated 1,3-diones and X-ray structure of 3.