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. 2014 Sep 26;6(1):816–825. doi: 10.1039/c4sc01711k

Table 4. Selected NMR data of the compounds 17 a .

Compound 17a 17b 17c
R Ph Mes t Bu
31P 1.3 1.7 15.0
11B –13.6 –8.1 –13.9
C1 27.7 31.6 21.5
C2 125.2 128.3 124.7
C3 132.1 128.4 131.1
C4 21.7 19.5 27.3
1-H 2.98 3.98/2.71 2.38
3-H 6.09 5.46 5.78
4-H 2.13 2.23/1.71 2.03
19F (o) –129.2 –125.5/–127.4/–128.6/–131.5 –124.0/–125.5/–129.8/–132.1
19F (p) –159.3 –158.0/–160.9 –157.4/–160.7
19F (m) –165.0 –164.7 (2F)/–165.2/–165.8 –163.0/–163.8/–164.0/–165.0

aIn CD2Cl2, chemical shifts in ppm, δ-scale.