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. 2017 Sep 11;7:11129. doi: 10.1038/s41598-017-11649-4

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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(a) Transmittance of TOCs vs. sonication time. Square orange points refer to UV wavelength (300 nm), while blue round points indicate visible (500 nm) wavelength. (b) Evolution of both elastic modulus (filled circles, left axis) and of relaxation rates (open symbols, right axis). Arrows are guides for the eyes. The shaded region underlines the sonication times during which gel structure forms.