Table 2.
Sample ID Species (n =3) |
Storagea | Origin | tR (min) (peak m/z 585 > 277) | S/N peak m/z 585 > 277 | S/N peak m/z 585 > 71 | S/N peak m/z 588 > 280 | Ion ratio (peak area m/z 71)/(peak area m/z 277) (average of n = 3) | BMAA (μg g−1 wet mussel homogenate) (average of n = 3) |
---|---|---|---|---|---|---|---|---|
A:1 BM1 | CC, RT | Europe (Scandinavia) | 4.17 | 254 | 9 | 2298 | 0.030 | 0.56 |
A:2 BM1 | CC, RT | Europe (Scandinavia) | 4.17 | 230 | 21 | 1910 | 0.044 | 0.59 |
A:3 BM1 | CC, RT | Europe (Scandinavia) | 4.17 | 206 | 21 | 1568 | 0.050 | 0.50 |
B:1 BM1 | CC, RT | Europe (Scandinavia) | 4.17 | 66 | 8 | 1804 | 0.040 | 0.29 |
B:2 BM1 | CC, RT | Europe (Scandinavia) | 4.17 | 71 | 7 | 1524 | 0.038 | 0.31 |
B:3 BM1 | CC, RT | Europe (Scandinavia) | 4.17 | 100 | 5 | 2315 | 0.037 | 0.28 |
C:1 BM2 | CC, RT | South America | 4.17 | 1315 | 74 | 1677 | 0.055 | 4.46 |
C:2 BM2 | CC, RT | South America | 4.17 | 934 | 156 | 1854 | 0.057 | 4.85 |
C:3 BM2 | CC, RT | South America | 4.17 | 876 | 93 | 1427 | 0.053 | 4.48 |
D:1 BM2 | CC, RT | South America | 4.17 | 936 | 107 | 1529 | 0.072 | 6.08 |
D:2 BM2 | CC, RT | South America | 4.17 | 1676 | 129 | 1112 | 0.064 | 6.98 |
D:3 BM2 | CC, RT | South America | 4.18 | 961 | 66 | 1284 | 0.057 | 6.52 |
E:1 BM2 | CC, RT | South America | 4.17 | 1221 | 77 | 1434 | 0.059 | 7.08 |
E:2 BM2 | CC, RT | South America | 4.17 | 2073 | 121 | 847 | 0.062 | 6.89 |
E:3 BM2 | CC, RT | South America | 4.17 | 1947 | 263 | 2026 | 0.060 | 6.93 |
F:1 BM2 | PB, F | South America | 4.17 | 534 | 29 | 1469 | 0.058 | 1.77 |
F:2 BM2 | PB, F | South America | 4.17 | 507 | 49 | 1372 | 0.068 | 2.28 |
F:3 BM2 | PB, F | South America | 4.17 | 316 | 58 | 1627 | 0.074 | 1.69 |
H:1 GM | PB, F | Australia | 4.17 | 531 | 17 | 1001 | 0.051 | 0.85 |
H:2 GM | PB, F | Australia | 4.17 | 243 | 22 | 2669 | 0.072 | 0.55 |
H:3 GM | PB, F | Australia | 4.17 | 374 | 21 | 1795 | 0.041 | 1.14 |
G:1 S | PB, F | North America | 4.18 | 452 | 49 | 2554 | 0.074 | 1.12 |
G:2 S | PB, F | North America | 4.17 | 608 | 30 | 2693 | 0.069 | 1.12 |
G:3 S | PB, F | North America | 4.17 | 354 | 36 | 2334 | 0.050 | 1.46 |
Storage: CC = Cooked and Canned, RT = Room temperature, PB = Plastic bag, F = Freezer.