| Crystal data |
| Chemical formula |
[Zn(C9H11N2S2)2]·0.5C6H7N |
|
M
r
|
534.57 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
98 |
|
a, b, c (Å) |
9.419 (2), 15.299 (4), 17.149 (4) |
| α, β, γ (°) |
88.871 (9), 83.914 (8), 75.766 (6) |
|
V (Å3) |
2381.8 (10) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.40 |
| Crystal size (mm) |
0.30 × 0.20 × 0.08 |
| |
| Data collection |
| Diffractometer |
AFC12K/SATURN724 |
| Absorption correction |
Multi-scan (ABSCOR; Higashi, 1995 ▸) |
|
T
min, T
max
|
0.549, 1 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
13748, 9827, 8634 |
|
R
int
|
0.037 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.053, 0.120, 1.14 |
| No. of reflections |
9827 |
| No. of parameters |
555 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.55, −0.81 |
