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A) Optimized disulfide rebridging reagents and resultant conjugates. Arsenous acids (IV); dibromopyridazinediones (V); alkynes (VI); allyl sulfones (VII). B) Synthesis of allyl sulfone. C) Modification of peptides with: a) equimolar reagents leading to mono‐functionalized peptide, and b) excess reagents forming multiply functionalized peptide.
