Table 2.

The key assay performance parameters in plasma and urine. Accuracy and imprecision (%CV) were determined over 3 days with 6 sets of QC samples analyzed on each consecutive day. Data listed were based on the QCs within the working range of the assay.

A: Key assay performance parameters in plasma
	Mean intra-batch		Mean inter-batch
	% Accuracy	%Imprecision	% Accuracy	% Imprecision
11OH-THC	93.0 – 103.2	1.5 – 7.3	95.7 – 102.8	2.2 – 5.7
CBN	96.4 – 105.8	1.4 – 5.5	98.5 – 103.8	2.4 – 5.5
CBG	93.8 – 104.2	1.0 – 4.7	95.5 – 102.0	2.5 – 3.4
THC	89.5 – 112.6	0.5 – 7.5	94.9 – 106.6	3.8 – 7.5
THCV	75.3 – 121.2	1.6 – 6.5	96.0 – 103.0	15.7 – 17.2
THC-COOH	94.3 – 114.3	1.9 – 7.6	97.4 – 108.6	3.0 – 6.4
THCV-COOH	86.3 – 103.9	2.2 – 8.3	92.6 – 101.6	3.7 – 7.5
CBD	93.9 – 104.6	1.0 – 6.8	97.3 – 102.9	2.7 – 5.7
CBC	88.4 – 114.0	1.6 – 5.0	90.2 – 97.5	3.1 – 6.6
CBDV	78.1 – 109.9	2.1 – 6.7	95.2 – 99.8	11.3 – 14.4
THC-C-gluc	89.2 – 110.3	0.8 – 8.8	92.3 – 102.5	5.6 – 7.3

B: Key assay performance parameters in urine
	Mean intra-batch		Mean inter-batch
	%Accuracy	%Imprecision	%Accuracy	%Imprecision
11OH-THC	93.7 – 105.1	1.8 – 13.7	96.8 – 100.2	4.9 – 9.9
CBN	88.6 – 105.0	3.3 -12.0	92.9 – 100.4	5.8 – 11.7
CBG	91.7 – 107.3	2.3 – 8.2	96.7 – 103	3.6 – 7.3
THC	91.9 – 101.8	0.9 – 9.2	94.7 – 100.5	2.3 – 8.1
THCV	84.9 – 100.0	2.6 – 8.1	88.3 – 93.7	4.9 – 7.5
THC-COOH	90.9 – 102.9	2.4 – 8.5	94.2 – 100.9	4.3 – 7.4
THCV-COOH	85.3 – 100.6	2.3 – 15.2	92.1 – 97.8	7.9 – 10.5
CBD	92.3 – 100.8	1.8 – 8.3	94.4 – 99.3	2.2 – 6.4
CBC	88.3 – 101.7	1.6 – 10.3	92.6 – 100.6	4.4 – 10.8
CBDV	85.3 – 98.0	2.6 – 9.6	85.8 – 93.8	4.5 – 9.0
THC-C-gluc	82.6 – 104.0	2.8 – 14.1	88.6 – 100.8	5.4 – 9.6