Table 2. Data collection and processing.

Diffraction source	SuperNova Dual, microfocus Cu (Nova)
Wavelength (Å)	1.54
Temperature (K)	130
Detector	Atlas CCD
Crystal-to-detector distance (mm)	56
Rotation range per image (°)	0.5
Exposure time per image (s)	80
Space group	P212121
a, b, c (Å)	24.50, 41.09, 65.18
α, β, γ (°)	90, 90, 90
Mosaicity (°)	1.3, 1.01, 2.28
Resolution range (Å)	34.76–2.30
R merge	0.08 (0.21)
Total No. of reflections	43577
No. of unique reflections	3229
Completeness (%)	90.1 (77.9)
Multiplicity	8.3 (5.4)
〈I/σ(I)〉	40.1 (7.9)
Overall B factor from Wilson plot (Å2)	38.04