Table 3.
Summary of data collection and refinement statistics
| Data collection | |
| Space group | P21212 |
| Cell dimensions (Å) | |
| a, b, c | 92.26, 201.46, 78.34 |
| Resolution (Å) | 40–2.35 (2.39–2.35)a |
| Rmerge | 0.072 (0.481) |
| I/σI | 21.5 (2.2) |
| Completeness (%) | 98.6 (98.2) |
| Unique reflections | 61,804 (3044) |
| Redundancy | 3.3 (3.1) |
| Refinement | |
| Resolution (Å) | 39.75–2.35 (2.5–2.35) |
| No. reflections | 58,410 (8677) |
| Rwork/Rfree | 0.225/0.264 (0.329/0.374) |
| No. atoms | |
| Protein | 8829 |
| Ligand/ion | 14 |
| Water | 212 |
| Mean B-factors (Å2) | 46.0 |
| R. M. S. deviations | |
| Bond lengths (Å) | 0.009 |
| Bond angles (°) | 1.5 |
| Ramachandran plot (%) | |
| Core | 87.7 |
| Allowed | 11.0 |
| Generously allowed | 1.3 |
| Disallowed | 0 |
a The numbers in parentheses refer to the highest-resolution shell.