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. Author manuscript; available in PMC: 2018 Jul 25.
Published in final edited form as: Biochemistry. 2017 Jul 11;56(29):3745–3753. doi: 10.1021/acs.biochem.7b00211

Table 1.

Data collection and refinement statistics.

FOXA2-DBD/DNA complex
Resolution range [Å] 33.64 – 2.796 (2.896 – 2.796)
Space group C 1 2 1
Unit cell (a, b, c, α, β, γ) 195.126, 71.932, 72.155, 90.0, 103.14, 90.0
Total reflections 178752 (17848)
Unique reflections 23535 (2364)
Multiplicity 7.5 (7.5)
Completeness [%] 96.80 (86.05)
Mean I/sigma(I) 18.52 (2.71)
Wilson B-factor 68.73
R-merge 0.1666 (3.753)
R-meas 0.1789
R-work 0.2298 (0.3499)
R-free 0.2811 (0.3964)
Number of non-hydrogen atoms 5425
 Macromolecules 5384
 Water 41
Protein residues 460
RMS (bonds) 0.005
RMS (angles) 1.05
Ramachandran favored [%] 91
Ramachandran outliers [%] 3.4
Clashscore 10.38
Average B-factor 69.40
 Macromolecules 69.50
 Solvent 58.70