Table 1. Crystallographic data and refinement statistics of SA50S in complex with lincomycin (SA50S–linc) and SA50S in complex with RB02 (SA50S–RB02). Values for the highest-resolution shells are in parentheses.
| SA50S–linc | SA50S–RB02 | |
|---|---|---|
| Crystal information | ||
| Space group | P6522 | P6522 |
| a = b [Å] | 280.8 | 279.8 |
| c [Å] | 873.5 | 873.3 |
| α,β,γ [°] | 90, 90, 120 | 90, 90, 120 |
| Diffraction data statistics | ||
| X-ray source (ESRF) | ID29, ID23–1 | ID29, ID23–1 |
| Wavelength [Å] | 0.971 | 0.971 |
| Number of crystals | 30 | 17 |
| Resolution [Å] | 50–3.64 (3.70–3.64) | 50–3.45 (3.51–3.45) |
| Observed reflections | 2230088 | 2863682 |
| Unique reflections | 223602 | 254888 |
| Redundancy | 10.0 (4.4) | 11.2 (3.6) |
| Completeness [%] | 98.0 (78.1) | 96.3 (72.8) |
| <I>/<σ(I)> | 9.08 (1.37) | 10.28 (1.36) |
| R-merge [%] | 23.7 (97.2) | 18.8 (77.2) |
| Refinement statistics | ||
| R-factor [%] | 18.74 | 19.00 |
| R-free [%] | 23.4 | 23.30 |
| rmsd bonds [Å] | 0.009 | 0.0086 |
| Rmsd angles [°] | 1.438 | 1.388 |