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. Author manuscript; available in PMC: 2018 Aug 1.
Published in final edited form as: Anal Bioanal Chem. 2017 Jun 19;409(21):5019–5029. doi: 10.1007/s00216-017-0446-z

Table 2.

Analysis of steroid hormones in stranded code-1 Tursiops truncatus (animal SC1426) blubber using two liquid chromatography separation techniques

Analyte Biphenyl (n = 3)
C18 (n = 3)
LOD (ng/g) LOQ (ng/g) Mean (ng/g) Stdev RSD (%) LOD (ng/g) LOQ (ng/g) Mean (ng/g) Stdev RSD (%)
11-Deoxycortisol 0.181 0.240 0.924 0.134 14.5 0.074 0.240 0.621 0.103 16.6
17-OH-Progesterone 0.0580 0.237 1.42 0.14 10.2 0.221 0.839 1.38 0.25 18.4
Androstenedione 0.0667 0.238 2.00 0.23 11.5 0.216 0.464 1.96 0.22 11.2
Corticosterone 0.128 0.252 1.40 0.16 11.5 0.0496 0.488 1.25 0.06 4.98
Cortisol 0.357 0.400 14.1 2.00 14.4 0.263 0.400 10.2 0.60 5.84
Cortisone 0.339 0.821 9.08 0.41 4.60 0.140 0.821 5.82 0.10 1.67
Progesterone 0.132 0.247 1.96 0.20 9.90 0.229 0.398 1.82 0.32 17.9
Testosterone 0.0735 0.236 2.74 0.16 5.80 NQ 0.838 2.31 0.94 40.8

NQ: Not quantifiable