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Top: Electronic absorption spectrum resulting from the NO(g) reactivity with 1 mM [CuI(tmpa)(MeCN)]+ in MeOH at RT. Bottom: EPR spectra (experimental (green) and simulated (red)) of [{CuII(tmpa)}2(μ-N2O22−)]2+ (2 mM in MeOH/EtOH = 1:1 glass) at 20 K (g⊥ = 2.18, g|| = 1.99; A⊥ = 82 G, A|| = 90 G).
