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Comparison of previously reported first-generation catalytic systems (alkyl iodides)9 with current protocol (alkyl bromides).
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Reactions of alkyl iodides as reported in ref. 9. All reactions of alkyl bromides were performed with [substrate]0 = 0.25 M in PhCF3 at 100 °C with 5 mol % [Pd(allyl)Cl]2, 20 mol % dtbpf, and 2 equiv Et3N as base.
Isolated yield.
Isolated with minor regioisomers, see Supporting Information for details.
