Table 1.

Characteristics of T85-LPEI (Z polymers)

Code	Composition (Molar Ratio)a	N (%)b	Mw (Da)		PEI (%)d	Grafted T85 /PEIb
			EAb	1H NMRc
Z0	T85	0			0
Z1	T85-PEI 0.8k (1:1)	4.43	6,019.6	6,981.4	13.28	6.53
Z2	T85-PEI 0.8k (1:3)	5.20	5,123.5	5,534.8	15.61	5.40
Z3	T85-PEI 0.8k (3:1)	4.12	6,422.5	7,223.6	12.46	7.02
Z4	T85-PEI 1.2k (1:1)	5.17	7,766.7	8,370.2	15.45	5.47
Z5	T85-PEI 1.2k (1:3)	6.24	6,410.3	5,796.3	18.72	4.34
Z6	T85-PEI 1.2k (3:1)	4.65	8,602.2	9,289.4	13.95	6.17
Z7	T85-PEI 2.0k (1:1)	2.85	23,391.8	25,863.7	8.55	10.70
Z8	T85-PEI 2.0k (1:3)	6.97	9,564.8	10,808.3	20.91	3.78
Z9	T85-PEI 2.0k (3:1)	2.75	24,242.5	29,485.6	8.25	11.12
Z8-PMOe	conjugate	about three PMOs were grafted onto one Z8 polymer

^aFeed ratio of starting materials

^bMicroanalysis of nitrogen

^c1H-NMR analysis with 500 MHz Jeol

^dAssume the N (%) is 33.33 WT% in each PEI

^ePMO covalent to polymer chemically