Table 2. Crystallographic data collection and refinement statistics.
| F80Y | F80M | F83M | T114S | |
|---|---|---|---|---|
| Data collection | PDB 6B24 | PDB 6B2A | PDB 6B2B | PDB 6B2D |
| Spacegroup | P41 | P41 | P41 | P41 |
| Cell dimensions | ||||
| a, b, c (Å) | 88.4, 88.4, 146.1 | 87.3, 87.3, 143.2 | 87.0, 87.0, 141.4 | 87.1, 87.1, 143.9 |
| a, b, g (°) | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 |
| Resolution (Å) | 42.7–2.75 (2.90–2.75) | 43.7–2.65 (2.78–2.65) | 47.1–2.60 (2.72–2.60) | 37.8–3.01 (3.19–3.01) |
| Rmeas | 0.111 (1.40) | 0.099 (1.52) | 0.107 (1.98) | 0.106 (1.57) |
| I/σ | 11.2 (1.5) | 14.4 (1.5) | 15.0 (1.5) | 14.1 (1.5) |
| CC1/2 | 0.998 (0.714) | 0.997 (0.667) | 1.00 (0.662) | 0.999 (0.707) |
| Completeness | 95.9 (97.2) | 100 (100) | 99.9 (99.9) | 99.8 (99.6) |
| Multiplicity | 10.1 (9.5) | 9.9 (8.7) | 12.9 (13.2) | 8.7 (8.9) |
| Refinement Statistics | ||||
| Resolution (Å) | 42.7–2.75 | 43.7–2.65 | 47.1–2.60 | 37.8–3.01 |
| No. Reflections | 26553 | 29629 | 30718 | 20151 |
| Rwork/Rfree | 0.225/0.251 | 0.225/0.243 | 0.221/0.250 | 0.238/0.254 |
| Ramachandran Favored | 0.97 | 0.97 | 0.97 | 0.97 |
| Ramachandran Outliers, % | 0 | 0 | 0.2 | 0 |
| RMS deviations | ||||
| Bond Lengths (Å) | 0.0076 | 0.0072 | 0.0070 | 0.0065 |
| Bond Angles (°) | 1.10 | 1.12 | 1.13 | 1.03 |