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. 2017 Oct 11;7:12954. doi: 10.1038/s41598-017-13472-3

Table 2.

Optimization of the catalyst.

Entry Catalyst DFE yield (%) Entry Catalyst DFE yield (%)
1 4a 2.08 10 4j 7.62
2 4b 5.41 11 4k 6.46
3 4c 7.85 12 4 l 1.41
4 4d 13.30 13 4 m 17.92
5 4e 3.55 14 4n 16.46
6 4 f 3.97 15 4o 16.73
7 4 g 4.90 16 4p 14.06
8 4 h 14.58 17 4q 14.20
9 4i 13.09 18 4r 26.90

*Reaction conditions: FA (10 mmol), catalyst (0.1 mmol), toluene (10 mL), 100 °C and 7 h. GC yield.