. 2017 Oct 12;12(10):e0186020. doi: 10.1371/journal.pone.0186020

Table 3. Mortality of S. oryzae adults exposed to selected four phytocompounds at different concentrations and times under with and without-food conditions.

Condition	Compounds	Concentration (μl/L air)
Condition	Compounds	20	100	200	400
Without-food	24 h treatment
	Eucalyptol	0.00 ± 0.00^a	9.09 ± 6.38^a	87.88 ± 5.88^c	95.96 ± 4.03^d
	N. Menthol^*	0.00 ± 0.00^a	5.05 ± 2.47^a	9.09 ± 4.51^a	11.11 ± 5.88^ab
	Menthone	0.00 ± 0.00^a	1.01 ± 2.02^a	3.03 ± 4.03^a	7.07 ± 3.77^a
	M. Acetate^#	15.15 ± 6.04^b	21.21 ± 8.67^a	39.39 ± 5.52^b	47.47 ± 4.94^c
	Phosphine	0.00 ± 0.00^a	6.00 ± 2.45^a	12.00 ± 3.74^a	32.00 ± 3.16^bc
	48 h treatment
	Eucalyptol	0.00 ± 0.00^a	53.54 ± 5.14^d	100.0 ± 0.00^c	100.0 ± 0.00^c
	N. Menthol^*	7.07 ± 5.88^ab	13.13 ± 2.47^a	23.23 ± 5.14^a	27.27 ± 3.77^a
	Menthone	0.00 ± 0.00^a	37.37 ± 5.88^bc	71.72 ± 7.41^b	95.96 ± 2.47^c
	M. Acetate^#	19.19 ± 4.51^b	23.23 ± 4.03^ab	59.60 ± 3.19^b	61.62 ± 11.67^b
	Phosphine	8.00 ± 5.82^ab	32.00 ± 3.74^ab	52.00 ± 5.82^b	66.00 ± 3.99^b
	72 h treatment
	Eucalyptol	10.20 ± 9.88^a	69.39 ± 3.22^b	100.0 ± 0.00^c	100.0 ± 0.00^b
	N. Menthol^*	14.29 ± 8.28^a	32.65 ± 6.91^a	42.86 ± 2.49^a	51.02 ± 4.99^a
	Menthone	28.57 ± 7.20^a	65.31 ± 5.19^b	100.0 ± 0.00^c	100.0 ± 0.00^b
	M. Acetate^#	36.73 ± 7.48^a	51.02 ± 5.94^ab	69.39 ± 4.56^b	87.76 ± 4.99^b
	Phosphine	13.13 ± 2.47^a	65.66 ± 5.14^b	73.74 ± 2.47^b	85.86 ± 4.03^b
With-food	24 h treatment
	Eucalyptol	0.00 ± 0.00^a	0.00 ± 0.00^a	9.09 ± 5.52^a	89.89 ± 7.81^c
	N. Menthol^*	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a
	Menthone	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a
	M. Acetate^#	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a
	Phosphine	2.00 ± 2.00^a	8.00 ± 3.74^a	34.00 ± 5.09^a	42.00 ± 5.82^b
	48 h treatment
	Eucalyptol	0.00 ± 0.00^a	5.05 ± 4.03^a	31.31 ± 5.88^c	97.98 ± 2.02^d
	N. Menthol^*	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a	0.00 ± 0.00^a
	Menthone	0.00 ± 0.00^a	11.11 ± 3.77^a	55.56 ± 2.47^d	73.74 ± 4.03^c
	M. Acetate^#	3.30 ± 2.49^a	7.07 ± 2.02^a	15.15 ± 4.03^b	21.21 ± 3.77^b
	Phosphine	6.00 ± 2.45^a	40.00 ± 4.46^b	48.00 ± 3.74^d	62.00 ± 5.82^c
	72 h treatment
	Eucalyptol	6.12 ± 3.81^a	24.49 ± 9.45^b	87.75±4.99^cd	100.0 ± 0.00^c
	N. Menthol^*	0.00 ± 0.00^a	0.00 ± 0.00 ^a	0.00 ± 0.00^a	0.00 ± 0.00^a
	Menthone	14.29 ± 5.19^a	42.86 ± 6.91^bc	100.0 ± 0.00^d	100.0 ± 0.00^c
	M. Acetate^#	8.16 ± 3.22^a	28.57 ± 1.77^b	38.78 ± 4.56^b	42.86 ± 8.28^b
	Phosphine	16.00 ± 5.09^a	68.00 ± 6.62^c	80.00 ± 4.46^c	88.00 ± 2.00^c

*Neoisocarvomenthol;

^#Menthyl acetate;

Each value is a mean of five replicates with standard error (Mean ± SE). Means within a column and within exposure period (h) followed by the different letters are significantly different (P≤0.05) of mortality of S. oryzae adults as determined by Tukey’s test.