Table 2. Results of the O-ATRP of MMA Investigating PC 4 Loading^a.

run. no.	[PC 4] (mol %)	conv (%)b	Mn (kDa)c	Đ (Mw/Mn)c	theor Mn (kDa)d	I* (%)e
1	0.1	61	6.4	1.23	6.11	95
2	0.04	69	6.9	1.22	6.86	100
3	0.02	68	6.2	1.26	6.82	110
4	0.01	71	7.9	1.27	7.09	90
5	0.005	72	6.7	1.60	7.25	108

^a[MMA]:[DBMM]:[4] = [1000:[10]:[X]; 2:3 of MMA to DMA by volume and 160 cm tubing reactor irradiated by 3000 K fluorescent lamp. Results shown were achieved with a 90 min residence time at a flow rate of 8.11 μL/min.

^bDetermined by ¹H NMR.

^cMeasured using GPC.

^dCalculated by (Conv × [Mon]/[Init] × M_w,Mon)/1000.

^eInitiator efficiency (I*) calculated by (Theor M_n/Calcd M_n) × 100.