Table 2.
X-ray Data collection and processing statistics. Values in parentheses are for the highest resolution shell.
| Dataset | Native | K2PtCl4 | K2PtCl6 | Co-crystal with 10 mM lactate |
|---|---|---|---|---|
| Space group | C2 | P321 | P321 | C2 |
| a, b, c (Å) | 189.3, 103.2, 61.8 | 102.7, 102.7, 62.4 | 102.5, 102.5, 63.0 | 188.5, 102.6, 61.2 |
| β (°) | 98.3 | 98.5 | ||
| Resolution range (Å) | 30.6–2.2 | 62.4–3.3 | 51.4–3.3 | 30.0–2.5 |
| (2.31–2.20) | (3.48–3.30) | (3.48–3.30) | (2.60–2.50) | |
| Rmerge | 0.062 (0.280) | 0.095 (0.364) | 0.096 (0.302) | 0.069 (0.341) |
| Average I/σ(I) | 13.3 | 18.2 | 18.1 | 58.5 |
| Completeness (%) | 98 (96) | 99.9 (99.9) | 99.9 (99.9) | 99.8 (99.9) |
| Redundancy | 3.6 | 10.5 | 10.5 | 3.6 |
| Anomalous redundancy | 5.5 | 5.4 | ||
| Observed reflections | 215,101 | 62,341 | 62,541 | 505,592 |
| Unique reflections | 59,028 | 5,941 | 5,975 | 40,012 |