Table 5.
X-ray data and refinement statistics
| Data collection | |
| Space group | P6522 |
| Unit cell | a = 65.1 Å, |
| c = 477.6 Å | |
| Resolution (Å) | 2.65 |
| Measured reflections | 584,843 |
| Unique reflections | 18,054 |
| Redundancy | 13.1 |
| Completeness (%, highest shell) | 95.4 (97.9) |
| Mean I/σI (highest shell) | 50.6 (2.3) |
| Rsym (%, highest shell) | 0.107 (0.000) |
| Refinement | |
| Resolution (Å) | 2.65 |
| No. of reflections |F|>0 σF | 18,043 |
| R-factor/R-free (%) | 26.0/29.8 |
| No. of atoms | |
| Protein | 3,323 |
| Carbohydrate | 196 |
| Water | 94 |
| Root mean square deviations | |
| Bond lengths (Å) | 0.009 |
| Bond angles (°) | 1.176 |
| Ramachandran plot | |
| Most favored regions (%) | 95.4 |
| Additional allowed regions (%) | 3.1 |
| Generously allowed regions (%) | 0.5 |
| Disallowed regions (%) | 0.0 |