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. 2017 Nov 1;7:14851. doi: 10.1038/s41598-017-14782-2

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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In situ HCl test of G-SERS. Time-resolved surface-enhanced Raman spectra of (A) Ag/SiO₂/Si and (B) G-SERS at 60 s interval in diluted HCl solution. The concentration of the HCl was 1 × 10⁻⁵ M. (C) Normalized intensities at 1600 cm⁻¹ (blue) in (A) Ag/SiO₂/Si and of G’ peak (red) in (B) G-SERS with respect to time after immersing in HCl.