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. 2017 Nov 7;7:14688. doi: 10.1038/s41598-017-15319-3

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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(a,d) TG curve of pre-cal pPTND3 and pre-cal PTND3; (b,c) IR spectra curves of apPTND3 (pPTND3 adsorbed NH₃) and dpPTND3 (pPTND3 desorbed NH₃); (e,f) IR spectra curves of PTND3, aPTND3 (PTND3 adsorbed NH₃) and dPTND3 (aPTND3 desorbed NH₃) (RT: 26 °C, humidity of 30%, synthesis and treatment conditions of above mentioned samples see in Table S1).