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Molecular structures of [Si15-LLA17] (A) and [Si7-M33] (B). (C) DSC traces of [Si15-LLA17] (black) and [Si7-M33] (red). The data are shifted vertically for clarity. The order–disorder transition unrelated to the crystallization process is indicated with an asterisk. (D) Room-temperature SAXS data for discrete [Si15-LLA17] (top) and [Si7-C33] (bottom). The data are shifted vertically for clarity. A selection of higher order reflections is indicated.
