Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

	PhyH-DI	SeMet PhyH-DI
Diffraction source	3W1A, BSRF	3W1A, BSRF
Wavelength (Å)	1.0000	0.9792
Temperature (K)	100	100
Detector	MAR CCD	MAR CCD
Crystal-to-detector distance (mm)	180	180
Rotation range per image (°)	1	1
Total rotation range (°)	243	1080
Exposure time per image (s)	90	45
Space group	C121	C2221
a, b, c (Å)	156.84, 45.54, 97.64	94.71, 97.03, 69.16
α, β, γ (°)	90.00, 125.86, 90.00	90.00, 90.00, 90.00
Mosaicity (°)	1.489	0.858
Resolution range (Å)	50.0–3.00 (3.05–3.00)	50.00–2.70 (2.75–2.70)
Total No. of reflections	58014	376627
No. of unique reflections	11541	8935
Completeness (%)	99.8 (100)	99.9 (99.3)
Multiplicity	5.0 (5.0)	41.6 (31.2)
〈I/σ(I)〉	9.61 (2.49)	21.16 (3.38)
R r.i.m. (%)	20.01 (70.88)	20.95 (68.63)
Overall B factor from Wilson plot (Å2)	41.0	44.2