Table 3.

Crystallographic statistics.

Wavelength	1 Å
Resolution range	41.9-1.92(1.99-1.92)
Space group	C 1 2 1
Unit cell	85.13 48.75 55.80 90 105.97 90
Total reflections	16652
Unique reflections	16650(1447)
Multiplicity	7.0(5.1)
Completeness (%)	96.1(79.9)
Mean I/sigma(I)	21.7
Wilson B-factor	28.2
R-meas	0.077(0.339)
R-pim	0.032(0.141)
Reflections used in refinement	16259(1337)
Reflections used for R-free	1616(133)
R-work	0.187(0.236)
R-free	0.240(0.313)
Number of non-hydrogen atoms	1824
macromolecules	1646
solvent	178
Protein residues	200
RMS(bonds)	0.006
RMS(angles)	0.75
Ramachandran favored (%)	97.4
Ramachandran allowed (%)	2.1
Ramachandran outliers (%)	0.5
Rotamer outliers (%)	0.5
Clashscore	6.8
Average B-factor	42.0
macromolecules	41.9
solvent	43.7
Number of TLS groups	8

Statistics for the highest-resolution shell are shown in parentheses.