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. Author manuscript; available in PMC: 2017 Nov 20.
Published in final edited form as: Inorg Chem. 2017 Nov 7;56(22):14118–14128. doi: 10.1021/acs.inorgchem.7b02230

Figure 6.

Figure 6

EPR spectra (red) and simulations (black) of [NiII(OH)FeIII]+ at the temperatures listed, showing changes in the relative intensities of the signals (g = 5.45, 5.05, 2.34, 1.65) from the SC = 3/2 state and growth of the g = 8 signal from the SC = 5/2 state. Microwave parameters: 9.663 GHz, 0.2 mW, B1 ⊥ B. The simulations matched the temperature dependence of the signals and used a concentration that was in quantitative agreement with that measured for the complex.