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. Author manuscript; available in PMC: 2018 Jun 16.
Published in final edited form as: Anal Methods. 2017 Jun 16;9:3876–3883. doi: 10.1039/C7AY00532F

Table 2.

Accuracy and precision for QC samples and lowest calibrator, N=20.

Lowest Calibrator (1.0 ng/mL) QC Low (7.5 ng/mL) QC High (75 ng/mL)

% RSD % Error % RSD % Error % RSD % Error

Fentanyl* 9.5 −7.8 6.6 −2.3 5.1 −4.1
Sufentanil* 11 −6.3 9.8 −7.4 6.5 −4.9
Carfentanil* 14 −8.3 11 −7.4 6.4 −5.9
Alfentanil* 10 −9.1 6.8 −4.4 6.6 −3.6
Lofentanil 16 −4.3 15 −5.6 15 −4.2
α-methyl fentanll 25 −5.0 24 −4.6 19 −7.2
3-methyl fentanil 20 −2.3 21 −5.3 18 −5.3
*

Represents analogs with isotopically labeled matched internal standards.