Table 7.
Volumes of aqueous hydrochloric acid solution, sodium hydroxide solution, and calculated deacetylation degree values obtained for COSB samples (n = 6).
Sample * | G (g) | VHCl | VNaOH | DD (%) | (%) | RSD (%) |
---|---|---|---|---|---|---|
1-1 | 0.50018 | 18.00 | 20.00 | 93.28 | 92.59 | 0.53 |
1-2 | 0.50022 | 18.00 | 20.21 | 92.23 | ||
1-3 | 0.50038 | 18.00 | 20.25 | 92.00 | ||
1-4 | 0.50001 | 18.00 | 20.05 | 93.07 | ||
1-5 | 0.50051 | 18.00 | 20.15 | 92.48 | ||
1-6 | 0.50042 | 18.00 | 20.15 | 92.49 |
G: weight of COSB sample; VHCl: volume of standard aqueous HCl solution (mL); VNaOH: volume of standard NaOH aqueous solution (mL); * Moisture value of analyzed samples is 5.8% for COSB.