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. 2017 Apr 27;53(38):5334–5337. doi: 10.1039/c7cc01407d

Table 2. Synthesis of 1A, 4A, 1B, 1C, 5C and 6C.

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Amine Grignard reagent Solvent Product Yield (%)
graphic file with name c7cc01407d-u3.jpg graphic file with name c7cc01407d-u4.jpg MeCN graphic file with name c7cc01407d-u5.jpg 46
graphic file with name c7cc01407d-u6.jpg graphic file with name c7cc01407d-u7.jpg MeCN graphic file with name c7cc01407d-u8.jpg 0
graphic file with name c7cc01407d-u9.jpg graphic file with name c7cc01407d-u10.jpg MeCN graphic file with name c7cc01407d-u11.jpg 0
graphic file with name c7cc01407d-u12.jpg graphic file with name c7cc01407d-u13.jpg MeCN graphic file with name c7cc01407d-u14.jpg 37
graphic file with name c7cc01407d-u15.jpg graphic file with name c7cc01407d-u16.jpg MeCN graphic file with name c7cc01407d-u17.jpg 57
graphic file with name c7cc01407d-u18.jpg graphic file with name c7cc01407d-u19.jpg Et2O graphic file with name c7cc01407d-u20.jpg 28
graphic file with name c7cc01407d-u21.jpg graphic file with name c7cc01407d-u22.jpg Et2O graphic file with name c7cc01407d-u23.jpg 19
graphic file with name c7cc01407d-u24.jpg graphic file with name c7cc01407d-u25.jpg Et2O graphic file with name c7cc01407d-u26.jpg 5