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. 2017 Dec 5;7:16984. doi: 10.1038/s41598-017-17111-9

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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TEM analysis of a FIB section through a bipyramidal mineral from S. acidocaldarius mineralized for 24 h and heated for 1 day at 150 °C in close system. STEM (A) and TEM (B) images of the section and corresponding SAED pattern consistent with lipscombite. (C,D) EDX map and spectra of the area in (B). Colours of the spectra correspond to regions of interest of the same colour in (C). Arrowhead in panel A shows a large ovoid possibly resulting from the coalescence of individual cellular residues.