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(a) Superposition of the 2D version of the 13C-filtered NOESY-HSQC (red, 80 ms mixing time) and the 1H,13C-CT-HSQC (grey) spectra of the CV-N/Man3 complex. (b) Side-chain region of the 1H,13C-HSQC-NOESY spectrum of the CV-N/Man3 complex (60 ms mixing time). Intermolecular NOEs between sugar ring protons (correlated through 13C in f1) and protein side-chain protons are labeled.
