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. Author manuscript; available in PMC: 2018 May 3.
Published in final edited form as: J Am Chem Soc. 2017 Apr 21;139(17):6210–6216. doi: 10.1021/jacs.7b01929

Figure 4.

Figure 4

(a) Amide proton region of the 1H,13C-HSQC-NOESY spectrum (60 ms mixing time) of the CV-N/Man3 complex. Intermolecular NOEs between sugar ring protons and protein amide protons are labeled. (b) 1H,15N 2D version of the CNH-NOESY experiment (red, 20 ms mixing time) superimposed onto a 1H,15N-HSQC spectrum (grey). Amide proton resonances exhibiting NOEs to 13C-attached sugar ring protons are connected by dashed lines.