| Rigaku R-AXIS RAPIDII diffractometer | 2537 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.021 |
| ω scans | θmax = 30.0°, θmin = 3.3° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −21→21 |
| Tmin = 0.896, Tmax = 0.949 | k = −5→4 |
| 17752 measured reflections | l = −24→24 |
| 2789 independent reflections |
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