Table 1. Hydrogen-bond geometry (Å, °) for (I) .
D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
---|---|---|---|---|
N1—H1⋯O5A | 0.895 (17) | 1.843 (17) | 2.7380 (19) | 179 (2) |
N1—H1⋯O5B | 0.895 (17) | 1.907 (17) | 2.7417 (18) | 154 (2) |
O2—H2⋯O5B | 0.83 (3) | 2.12 (3) | 2.8111 (19) | 141 (3) |
O3—H3⋯O3i | 0.82 (3) | 1.62 (4) | 2.4352 (14) | 174 (4) |
O5A—H9A⋯O4ii | 0.82 (3) | 2.11 (3) | 2.927 (2) | 170 (3) |
O5B—H9B⋯O4ii | 0.82 (3) | 2.02 (3) | 2.8159 (19) | 162 (3) |
O5A—H10A⋯O2 | 0.84 (3) | 1.90 (3) | 2.6762 (19) | 154 (4) |
O5B—H10B⋯O1iii | 0.85 (2) | 2.60 (3) | 3.095 (2) | 119 (2) |
C8—H8⋯Cl1iii | 0.95 | 2.78 | 3.6524 (12) | 154 |
C8—H8⋯O1iii | 0.95 | 2.47 | 3.1871 (14) | 132 |
Symmetry codes: (i) ; (ii) ; (iii) .